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Analysis of salicylic acid using square-wave voltammetry with preconcentrationby solid phase extraction onto magnetite nanoparticles |
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| รหัสดีโอไอ | |
| Creator | Phetlada Sanchayanukun |
| Title | Analysis of salicylic acid using square-wave voltammetry with preconcentrationby solid phase extraction onto magnetite nanoparticles |
| Contributor | Prapanee Pengmarerng, Sasithorn Muncharoen |
| Publisher | Nakhon Pathom Rajabhat University |
| Publication Year | 2562 |
| Journal Title | Journal of Thai Interdisciplinary Research |
| Journal Vol. | 14 |
| Journal No. | 1 |
| Page no. | 35 |
| Keyword | salicylic acid, nano-magnetic particles, solid phase extraction, square-wave voltammetry, pencil leadelectrode |
| URL Website | http://rdi.npru.ac.th |
| Website title | วารสารวิจัยสหวิทยาการไทย |
| ISSN | 2465-3837 |
| Abstract | A pencil lead electrode coupling with nano-magnetite adsorption as pre-concentration and extraction in order toanalyze salicylic acid (SA) was demonstrated in this work. The optimum conditions for nano-magnetite (Fe3O4)preparation by co-precipitation of ferrous/ferric ions were studied. The parameters affecting the shape and size of thenano-magnetite particles such as the types of base, addition rate, temperature, stirring rate and pH were optimized.The morphology was characterized by Fourier transform infrared spectroscopy, energy dispersive X-ray spectroscopyand transmission electron microscopy. The application of nano-magnetite as the solid phase extractor for the squarewavevoltammetry (SWV) of SA gave good results. |