Analysis of salicylic acid using square-wave voltammetry with preconcentrationby solid phase extraction onto magnetite nanoparticles
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Creator Phetlada Sanchayanukun
Title Analysis of salicylic acid using square-wave voltammetry with preconcentrationby solid phase extraction onto magnetite nanoparticles
Contributor Prapanee Pengmarerng, Sasithorn Muncharoen
Publisher Nakhon Pathom Rajabhat University
Publication Year 2562
Journal Title Journal of Thai Interdisciplinary Research
Journal Vol. 14
Journal No. 1
Page no. 35
Keyword salicylic acid, nano-magnetic particles, solid phase extraction, square-wave voltammetry, pencil leadelectrode
URL Website http://rdi.npru.ac.th
Website title วารสารวิจัยสหวิทยาการไทย
ISSN 2465-3837
Abstract A pencil lead electrode coupling with nano-magnetite adsorption as pre-concentration and extraction in order toanalyze salicylic acid (SA) was demonstrated in this work. The optimum conditions for nano-magnetite (Fe3O4)preparation by co-precipitation of ferrous/ferric ions were studied. The parameters affecting the shape and size of thenano-magnetite particles such as the types of base, addition rate, temperature, stirring rate and pH were optimized.The morphology was characterized by Fourier transform infrared spectroscopy, energy dispersive X-ray spectroscopyand transmission electron microscopy. The application of nano-magnetite as the solid phase extractor for the squarewavevoltammetry (SWV) of SA gave good results.
Journal of thai interdiscipinary research

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