Recovery of valuable metals from NMC-811 li-ion battery waste with froth flotation and hydrometallurgical extraction
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Creator 1. Saddam Husin
2. Aghni Ulma Saudi
3. Galih Taqwatomo
4. Muhammad Dikdik Gumelar
5. Jarot Raharjo
6. Sri Rahayu
7. Hariaman Prasetyo
8. Hanif Yuliani
9. Dita Adi Saputra
10. Oka Pradipta Arjasa
11. Agustanhakri
12. Wahyu Tri Utami
13. Hikam Angga Saputra
14. Annisa Ramadhanti Ririanza Putri
15. Anne Zulfia Syahrial
Title Recovery of valuable metals from NMC-811 li-ion battery waste with froth flotation and hydrometallurgical extraction
Publisher Faculty of Engineering, Khon Kaen University
Publication Year 2567
Journal Title Engineering and Applied Science Research
Journal Vol. 51
Journal No. 1
Page no. 117-127
Keyword Acid leaching, Froth flotation, Milling method, Nickel sulfate, Spent li-ion batteries, Solvent extraction
URL Website https://ph01.tci-thaijo.org/index.php/easr/index
Website title Engineering and Applied Science Research
ISSN 2539-6161
Abstract In this research, the primary objective is to study the recycling process of spent lithium-ion batteries (LIBs) for the recovery of valuable metals - specifically, nickel, manganese, and cobalt. This is accomplished through a comprehensive hydrometallurgical process that integrates froth flotation, acid leaching, and solvent extraction. The optimization of the flotation phase is a pivotal aspect of this study, with a focus on parameters like particle size and collector concentration. This optimization leads to a remarkable separation efficiency, evident in the recovery of 99.3% of the anode mass in the froth and 78.2% of the cathode mass in the precipitate. Notably, nickel emerges as the standout performer, with an extraordinary extraction efficiency of 99.97%. Nickel precipitates as an ammonium nickel sulfate crystals after solvent extraction due to supersaturation. These findings underscore the considerable potential of froth flotation and hydrometallurgical techniques as a sustainable, low-energy solution for recycling valuable metals sourced from spent LIBs.
Engineering and Applied Science Research

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