Extraction and Characterization of Cellulose Nanocrystals Produced by Acid Hydrolysis from Corn Husk
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Creator Piyaporn KAMPEERAPAPPUN
Title Extraction and Characterization of Cellulose Nanocrystals Produced by Acid Hydrolysis from Corn Husk
Publisher Metallurgy and Materials Science Research Institute, Chulalongkorn University
Publication Year 2558
Journal Title Journal of Metals, Materials and Minerals
Journal Vol. 25
Journal No. 1
Page no. 19-26
Keyword Corn husk,Cellulose nanocrystals,Acid-hydrolysis,Extraction
ISSN 8576149
Abstract Corn husk is one of the agricultural residues which are abundant, inexpensive, and readily available source of renewable lignocellulosic biomass. Cellulose nanocrystals (CNCs) were extracted from corn husk by alkali and bleaching treatments followed by sulfuric acid hydrolysis treatment. The material obtained after each stage of the treatments was characterized. Morphological investigation was carried out using scanning electron microscope (SEM) and transmission electron microscopy (TEM). Fourier transform infrared (FTIR) spectroscopy showed the progressive removal of non-cellulosic materials. The crystallinity of corn husk and CNCs was also investigated using X-ray diffraction analysis (XRD). The highest crystallinity index value of this study is 68.33% for cellulose nanocrystals.
Metallurgy and Materials Science Research Institute, Chulalongkorn University ​

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